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SYNTHESIS OF 2-[(3-SUBSTITUTEDIMINO)-1,2,4-DITHIAZOLO]AMINO-11-(PIPERAZIN-1-YL)DIBENZO [b,f][1,4]OXAZEPINES
Abstract
Recently in this laboratory a novel series of 2-[(3-substitutedimino)-1,2,4-dithiazolo]amino-11-(piperazin-1-yl)dibenzo [b,f][1,4]oxazepines [VIB(a-h)] was synthesized by the oxidative cyclisation of 2-[substituted-2,4-dithiobiureto]-11-(piperazin-1-yl) dibenzo [b,f] [1,4]oxazepines [VB(a-h)] in chloroform medium by making the use of liquid bromine as oxidizing agent. The products were characterized and justified on the basis of elemental analysis, chemical characteristics and spectral studies.
Keywords
Liquid bromine, 2-[substituted-2,4-dithiobiureto]-11-(piperazin-1-yl) dibenzo [b,f] [1,4]oxazepines and chloroform
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