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SYNTHESIS OF 2-[(3-SUBSTITUTEDIMINO)-1,2,4-DITHIAZOLO]AMINO-11-(PIPERAZIN-1-YL)DIBENZO [b,f][1,4]OXAZEPINES
Abstract
Recently in this laboratory a novel series of 2-[(3-substitutedimino)-1,2,4-dithiazolo]amino-11-(piperazin-1-yl)dibenzo [b,f][1,4]oxazepines [VIB(a-h)] was synthesized by the oxidative cyclisation of 2-[substituted-2,4-dithiobiureto]-11-(piperazin-1-yl) dibenzo [b,f] [1,4]oxazepines [VB(a-h)] in chloroform medium by making the use of liquid bromine as oxidizing agent. The products were characterized and justified on the basis of elemental analysis, chemical characteristics and spectral studies.
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